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Liberating the building blocks of quantum materials to create new devices

Researchers growing the building blocks of quantum devices on crystals have traditionally been stuck with the crystals. An interdisciplinary paper from UChicago Pritzker Molecular Engineering solves this pressing challenge.

Quantum materials, batteries and water might not seem like natural partners, but UChicago Pritzker School of Molecular Engineering (PME) experts in these three respective research fields have broken through a major barrier in creating new quantum devices.

“This is the perfect example of interdisciplinary research,” said PME Prof. Y. Shirley Meng, whose team contributed to the research.

One of the most common ways to build semiconductors, transistors, diodes and nanotechnology devices from the molecule up is a process called molecular-beam epitaxy (MBE). Researchers grow microscopically thin films of material on single crystal wafers called substrates.

The films can be sliced, diced and stacked in novel formations to create new devices on the microscopic level. The problem is that the valuable films are still stuck on – and stuck with – the substrates.

“Once the film is grown, it's permanently bonded to the substrate,” said PME Asst. Prof. Shuolong Yang, whose lab led the interdisciplinary team. “This puts some very strong limitations on how creative you can be in processing the material.”

In a paper published in Nano Letters, an interdisciplinary team from three PME labs has shown how MBE-grown films can be “liberated” from the substrates and still maintain their delicate quantum physics – an engineering triumph at the molecular level.

Peeling the tape

The ultrathin membranes created through MBE are the building blocks of exotic quantum materials. Researchers seeking to use these films to create new, innovative and better quantum devices came to see the substrates as an unavoidable burden, something that comes with the territory.

When an undergraduate student – Chi Ian Jess Ip, the new paper’s first author – approached Yang about potential research opportunities a few years ago, he presented this challenge and outlined the exciting future research opportunities if such a barrier could be overcome.

“She found a way to robustly separate topological insulator products, a form of material which is great for low-dissipation, low-power electronics,” Yang said.

Ip’s method, which is outlined in the paper, chemically removes the film where quantum properties previously deemed too delicate to survive being ripped off the substrate survived.

“We used an acid to selectively eat away the top few layers of atoms on the substrate, leaving the film floating on the acid and ready to be fished out by any other substrate or devices,” said Ip, now at MIT.

Ip’s teammates, postdoctoral scholar Qiang Gao and PhD student Duy Nguyen, led state-of-the-art electron spectroscopy studies which clearly resolved the quantum electronic states layer-by-layer.

“That’s the amazing part. There's lots of chemistry and acid and washing, but the quantum physics is somehow still preserved,” Yang said. “Spectroscopy showed that chemically removing the membrane damaged the outermost layer of atoms. But what's interesting is that the next layer inside becomes the de facto outer layer, preserving the membrane’s quantum properties.”

‘Fruitful collaboration’

A conversation with a colleague working in a completely different research area across the hall helped Yang’s team realize the full potential of Ip’s new technique.

That professor, PME Asst. Prof. Chong Liu, studies sustainable lithium extraction and other water-related issues. While casually discussing clean energy technology, Liu mentioned her lab’s recent insights on the ion exchange process.

Yang was struck by the similarities between the membranes his lab uses to create quantum materials and the membranes Liu’s lab uses to selectively extract metal ions from water. The pathways Yang team was using to create what he called “quantum highways” were similar to the general pathway Liu discovered in lithium and sodium ion exchange.

“I suddenly realized this was exactly what we were making in our lab,” Yang said.

Yang and Liu soon realized they needed a microscopy expert to study what was happening at the smallest level. They turned to Meng, whose Laboratory for Energy Storage and Conversion, primarily works on creating better batteries for the clean energy transition.

“We deployed some of the most advanced electron microscopy techniques for understanding the quantum materials, although our group traditionally work on energy materials,” Meng said.

Yang said this new research would not have been possible at institutions where research groups are isolated from each other.

“This is the kind of fruitful collaboration that UChicago PME hopes to facilitate,” Yang said. “While traditionally scientists live in their own territories, we realize there is a different way of thinking.”

Citation: “Preservation of Topological Surface States in Millimeter-Scale Transferred Membranes,” Ip, et al, Nano Letters, May 17, 2024. DOI: 10.1021/acs.nanolett.4c00008

Funding: This research is funded by DOE Basic Energy Sciences under Grant No. DE-SC0023317